Citation: | WU Bao-qiang, MA Xiao-xun, LIANG Bin, HAN Yun-da. Preparation of HZSM-5 zeolite assisted by glycerin and its catalytic performance for methane aromatization[J]. Journal of Fuel Chemistry and Technology, 2020, 48(7): 821-832. |
[1] |
NIKOLAY K, FERDY J A G C, GUANNA L, EVGENY U, BRAHIM M, ALEXANDRA S G W, EVGENYA P, EMIEL J M H. Stable Mo/HZSM-5 methane dehydroaromatization catalysts optimized for high-temperature calcination-regeneration[J]. J Catal, 2016, 346:125-133. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=e73abbacdffdf8b709ee4d4acf6a85ff
|
[2] |
黄鑫, 焦熙, 林明桂, 贾丽涛, 侯博, 李德宝.甲烷无氧直接制备芳烃研究进展[J].燃料化学学报, 2018, 46(9):1087-1100. http://manu60.magtech.com.cn/rlhxxb/CN/abstract/abstract19277.shtml
HUANG Xin, JIAO Xi, LIN Ming-gui, JIA Li-tao, HOU Bo, LI De-bao. Research progress in the direct nonoxidative dehydroaromatization of methane to aromatics[J]. J Fuel Chem Technol, 2018, 46(9):1087-1100. http://manu60.magtech.com.cn/rlhxxb/CN/abstract/abstract19277.shtml
|
[3] |
XU Y D, LIU S T, WANG L S. Methane activation without using oxi-dants over Mo/HZSM-5 zeolite catalysts[J]. Catal Lett, 1995, 30(1/4):135-149. doi: 10.1007/BF00813680
|
[4] |
WECKHUYSEN B M, WANG D J, ROSYNEK M P. Conversion of methane tobenzene over transition metal ion ZSM-5 Zeolites[J]. Catal, 1998, 175(2):338-346. https://www.sciencedirect.com/science/article/pii/S0021951798920103
|
[5] |
CHENG X, YAN P, ZHANG X, YANG F, DAI C, LI D, MA X. Enhanced methane dehydroaromatization in the presence of CO2 over Fe-and Mg-modified Mo/ZSM-5[J]. Mol Catal, 2017, 437:114-120. http://www.sciencedirect.com/science/article/pii/S2468823117302687
|
[6] |
马记源, 张航飞, 尹金莲, 周蓉, 陆江银. Ni改性Mo-Co/HZSM-5催化剂在甲烷无氧芳构化中的研究[J].天然气化工(C1化学与化工), 2016, 41(2):19-24. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=trqhg201602005
MA Ji-yuan, ZHANG Hang-fei, YIN Jin-lian, ZHOU Rong, LU Jiang-yin. Methane dehydroaromatization over Ni modified Mo-Co/HZSM-5 catalysts[J]. Nat Gas Ind, 2016, 41(2):19-24. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=trqhg201602005
|
[7] |
王冬杰.助催化剂对Mo/HZSM-5上甲烷无氧芳构化催化性能研究[D].杭州: 浙江大学, 2003. http://d.wanfangdata.com.cn/thesis/Y638762
WANG Dong-jie. Study on the catalytic performance of additive modified Mo/HZSM-5 catalysts for methane aromatization under O2-free condition[D]. Hangzhou: Zhejiang University, 2003. http://d.wanfangdata.com.cn/thesis/Y638762
|
[8] |
赵金凤. In、Pd助剂对Mo/HZSM-5催化剂上甲烷无氧芳构化改性的研究[D].大连: 中国科学院大连化学物理研究所, 2002. http://cdmd.cnki.com.cn/article/cdmd-80038-2002091858.htm
ZHAO Jin-ming. Study on the modification of Mo/HZSM-5 Catalyst by In and Pd promoters[D]. Dalian: University of Chinese Academy of Sciences, 2002. http://cdmd.cnki.com.cn/article/cdmd-80038-2002091858.htm
|
[9] |
XU C, GUAN J Q, WU S J, JIA M J, WU T H, KAN Q B. Catalystic performance of zeolite ITQ-13 with 9-and 10-member rings for methane dehydroaromation[J]. React Kinet Mech Catcd, 2010, 99:193-199. doi: 10.1007/s11144-009-0129-7
|
[10] |
WANG H, PINNAVAIA T J. MFI zeolite with small and uniform intracrystal mesopores[J]. Angew Chem Int Ed, 2006, 45:7603-7606. doi: 10.1002/anie.200602595
|
[11] |
XIAO F, WANG L, YIN C, LIN K, DI Y, LI J, XU R, SU D. Catalytic properties of hierarchical mesoporous zeolites templated with a mixture of small organic ammonium salts and mesoscale cationicpolymers[J]. Angew Chem Int Ed, 2006, 45:3090-3093. doi: 10.1002/ange.200600241
|
[12] |
王迪勇.多级结构ZSM-5分子筛的合成及甲烷无氧芳构化应用[D].大连: 大连理工大学, 2012. http://cdmd.cnki.com.cn/article/cdmd-10141-1012394366.htm
WANG Di-yong. The Synthesis of Hierarchical ZSM-5 Zeolite and the Performance in Methane Dehydroaromatization[D]. Dalian: Dalian University of Technology, 2012. http://cdmd.cnki.com.cn/article/cdmd-10141-1012394366.htm
|
[13] |
杨建华, 于素霞, 胡慧晔, 初乃波, 鲁金明, 殷德宏, 王金渠.无第二模板剂法合成多级结构ZSM-5分子筛微球及其在甲烷无氧芳构化反应中的应用[J].催化学报, 2011, 32(2):362-367. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=cuihuaxb201102025
YANG Jian-hua, YU Su-xia, HU Hui-ye, CHU Nai-bo, LU Jin-ming, YIN De-hong, WANG Jin-qu. Synthesis of hierarchical HZSM-5 microspheres without second template and their application in methane dehydroaromatization[J]. Chin J Catal, 2011, 32(2):362-367. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=cuihuaxb201102025
|
[14] |
王涛, 刘志玲, 张菊, 张媛, 张伟, 卢永斌.甲烷无氧芳构化反应最新研究进展[J].天然气化工(C1化学与化工), 2018, 43(2):127-134. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=trqhg201802026
WANG Tao, LIU Zhi-ling, ZHANG Ju, ZHANG Yuan, ZHANG Wei, LU Yong-bin. New advances in methane non-oxidative aromatization[J]. Nat Gas Ind, 2018, 43(2):127-134. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=trqhg201802026
|
[15] |
WANG L, TAO L, XIE M, XU G, HUANG J, XU Y. Dehydrogenation and aromatization of methane under non-oxidizing conditions[J]. Catal Lett, 1993, 21(1/2):35-41. doi: 10.1007%2FBF00767368
|
[16] |
ARGAUER R J, LANDOLTG R. Crystalline zeolite ZSM-5 and method of preparing the same: US, 3702886[P]. 1972.
|
[17] |
STANCIULESCU M, CARAVAGGIO G, DOBRI A, MOIR J, BURICH R, CHARLAND J P, BULSINK P. Low-temperature selective catalytic reduction of NOx with NH3 over Mn-containing catalysts[J]. Appl Catal B:Environ, 2012, 123-124:229-240. https://www.sciencedirect.com/science/article/abs/pii/S0926337312001476
|
[18] |
张伟, 张堃, 雍晓静, 王峰, 温鹏宇.不同硅源合成ZSM-5分子筛及其MTP反应催化性能[J].天然气化工(C1化学与化工), 2015, 40(1):13-17. http://www.cqvip.com/QK/94489X/201501/664081808.html
ZHANG Wei, ZHANG Kun, YONG Xiao-jing, WANG Feng, WEN Peng-yu. Effect of silica soures on synthesis of ZSM-5 and their catalytic properties for MTP reaction[J]. Nat Gas Ind, 2015, 40(1):13-17. http://www.cqvip.com/QK/94489X/201501/664081808.html
|
[19] |
李文林, 郑金玉, 罗一斌, 达志坚.多级孔分子筛制备方法、机理和应用研究进展[J].石油学报(石油加工), 2016, 32(6):1273-1286. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=syxb-syjg201606032
LI Wen-lin, ZHENG Jin-yu, LUO Yi-bin, DA Zhi-jian. Recent advances in preparation, mechanism and application of hierarchical zeolite[J]. Acta Petr Sin(Pet Process Sect), 2016, 32(6):1273-1286. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=syxb-syjg201606032
|
[20] |
胡雨, 杨雪, 田辉平.软模板法制备多级孔ZSM-5分子筛的研究进展[J].工业催化, 2020, 28(1):1-10. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=gych202001001
HU Yu, YANG Xue, TIAN Hui-ping. Research advance in synthesis hierarchical ZSM-5 zeolites with soft templates[J]. Ind Catal, 2020, 28(1):1-10. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=gych202001001
|
[21] |
刘宝玉.多级孔沸石的设计合成、催化性能及计算机模拟研究[D].广州: 华南理工大学, 2015. http://cdmd.cnki.com.cn/Article/CDMD-10561-1016706667.htm
LIU Bao-yu. Synthesis, catalytic property evaluation and computer simulation study of hierarchical zeolites[D]. Guangzhou: South China University of Technology, 2015. http://cdmd.cnki.com.cn/Article/CDMD-10561-1016706667.htm
|
[22] |
LI Y, YU J. New stories of zeolite structures:Their descriptions, determinations, predictions, and evaluations[J]. Chem Rev, 2014, 114(14):7268-316. doi: 10.1021/cr500010r
|
[23] |
VALTCHEV V, MAJANO G, MINTOVA S, JAVIER P R. Tailored crystalline microporous materials by post-synthesis modification[J]. Chem Soc Rev, 2013, 44(17):263-290. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=39d6779b59fbeec53fe060d3605e8436
|
[24] |
高敏, 刘春燕, 王刃, 郭洪臣.在含乙醇的硅铝凝胶中合成ZSM-5沸石[J].化学通报, 2009, 72(12):1097-1103. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=hxtb2200912008
GAO Min, LIU Chun-yan, WANG Ren, GUO Hong-chen. Synthesis of ZSM-5 zeolites from ethanol-containing aluminosilicate gels[J]. Chemistry, 2009, 72(12):1097-1103. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=hxtb2200912008
|
[25] |
STOCKER M. Methanol-to-hydrocarbons:Catalytic materials and their behavior[J]. Microporou Mesoporou Mater, 1999, 29:3-48. https://www.sciencedirect.com/science/article/pii/S1387181198003199
|
[26] |
OLSBYE U, SVELLE S, BJORGEN M, BEATO P, JANSSENS T V W, JOENSEN F, BORDIGA S, LILLERUD K P. Conversion of methanol to hydrocarbons:How zeolite cavity and pore size controls product selectivity[J]. Angew Chem Int Ed, 2012, 51:5810-5831. doi: 10.1002/anie.201103657
|
[27] |
孙洪满, 王有和, 尹寒梅, 许本静, 历阳, 阎子峰.模板剂法水热合成高硅铝比ZSM-5分子筛[J].硅酸盐通报, 2015, 34(4):1121-1126+1132. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=gsytb201504042
SUN Hong-man, WANG You-he, YIN Han-mei, XU Ben-jing, LI Yang, YAN Zi-feng.Synthesis of ZSM-5 zeolite with high molar ratio of silica to alumina by hydrothermal crystallization method with template[J]. Bull Chin Ceram Soc, 2015, 34(4):1121-1126+1132. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=gsytb201504042
|
[28] |
周浩, 付廷俊, 李忠.绿色合成ZSM-5分子筛的研究进展[J].天然气化工(C1化学与化工), 2015, 40(4):79-85. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=trqhg201504017
ZHOU Hao, FU Ting-jun, LI Zhong. Recent advance in green synthesis of ZSM-5 zeolite[J]. Nat Gas Ind, 2015, 40(4):79-85. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=trqhg201504017
|
[29] |
SEDEL NIKOVA O V, STEPANOV A A, ZAIKOVSKII V I, KOROBITSYNA L L, VOSMERIKOV A V. Preparation method effect on the physicochemical and catalytic properties of a methane dehydroaromatization catalyst[J]. Kinet Catal, 2017, 58(1):51-57. doi: 10.1134%2FS0023158417010074
|
[30] |
CHEN X, YAN W, SHEN W, YU J, CAO X, XU R. Morphology control of self-stacked silicalite-1 crystals using microwave-assisted solvothermal synthesis[J]. Microporous Mesoporous Mater, 2007, 104(1/3):296-304. https://www.sciencedirect.com/science/article/abs/pii/S1387181107002946
|
[31] |
龙英才.二乙醇胺-甘油-Na2O-SiO2-Al2O3-H2O系统中沸石的生成[J].化学学报, 1984, 42(6):523-528. http://www.cnki.com.cn/Article/CJFDTotal-HXXB198406004.htm
LONG Ying-cai. The crystallization of zeolites in diethanolamine-glycerol-Na2O-SiO2-Al2O3-H2O system[J]. Acta Chim Sin, 1984, 42(6):523-528. http://www.cnki.com.cn/Article/CJFDTotal-HXXB198406004.htm
|
[32] |
DENG Z, ZHANG Y, ZHENG J, ZHU K, ZHOU X. A hierarchical bulky ZSM-5 zeolite synthesized via glycerol-mediated crystallization using a mesoporous steam-treated dry gel as the precursor[J]. New J Chem, 2015, 39(10):7777-7780. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=580b0a2704947abeaec65744d2956c61
|
[33] |
徐如人, 庞文琴, 于吉红.分子筛与多孔材料化学[M].北京:科学出版社, 2004.
XU Ru-ren, PANG Wen-qin, YU Ji-hong. Molecular Sieve and Porous Material Chemistry[M]. Beijing:Science Press, 2004.
|
[34] |
刘宇, 韩顺玉, 曹翠萍, 张欢欢, 刘伟营, 姜男哲.甘油辅助下晶种法合成ZSM-5分子筛[J].石油学报(石油加工), 2018, 34(5):891-896. http://www.cqvip.com/QK/94167X/201805/7000829253.html
LIU Yu, HAN Shun-yu, CAO Cui-ping, ZHANG Huan-huan, LIU Wei-ying, JIANG Nan-zhe. Synthesis of ZSM-5 molecular sieve with glycerol assisted seed crystallization[J]. Acta Pet Sin, 2018, 34(5):891-896. http://www.cqvip.com/QK/94167X/201805/7000829253.html
|
[35] |
范素兵, 申达, 吕俊敏, 张建利, 赵天生.多级孔ZSM-5性质及其对甲醇制丙烯催化性能的影响[J].天然气化工(C1化学与化工), 2015, 40(1):1-5. http://d.wanfangdata.com.cn/periodical/trqhg2015010002
FAN Su-bing, SHEN Da, LV Jun-min, ZHANG Jian-li, ZHAO Tian-sheng. Properties of hierarchical ZSM-5 and its effect on reaction of methanol to propylene[J]. Nat Gas Ind, 2015, 40(1):1-5. http://d.wanfangdata.com.cn/periodical/trqhg2015010002
|
[36] |
尹建军, 邢伟静, 李玉波, 张佼, 张忠东, 高雄厚. ZSM-5分子筛结晶度及晶粒大小的影响因素[J].分子催化, 2012, 26(2):162-168. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=fzch201202012
YIN Jian-jun, XING Wei-jing, LI Yu-bo, ZHANG Jiao, ZHANG Zhong-dong, GAO Xiong-hou. The influence factors of the crystallinity and crystal size of ZSM-5 zeolite[J]. J Mol Catal A:Chem, 2012, 26(2):162-168. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=fzch201202012
|
[37] |
刘文艳, 王华, 高文桂, 张明宇, 张逢杰.不同助剂对合成甲醇工业催化剂二氧化碳加氢性能的影响[J].材料导报, 2012, 26(6):96-99. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=cldb201206026
LIU Wen-yan, WANG Hua, GAO Wen-gui, ZHANG Ming-yu, ZHANG Feng-jie. Effects of different promoters on the hydrogenation of carbon dioxide over catalysts for methanol synthesis[J]. Mater Rev, 2012, 26(6):96-99. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=cldb201206026
|
[38] |
RICHARD W B, YOUNG H K, ANNE H. Structure and density of Mo and acid sites in Mo-exchanged HZSM-5 catalysts for nonoxidative methane conversion[J]. J Phys Chem B, 1999, 103(28):5787-5796. http://iglesia.cchem.berkeley.edu/Publications/JPhysChemB_103_5787_1999.pdf
|
[39] |
杨平, 辛靖, 李明丰, 聂红.负载Mo、W氧化物对Y型分子筛结构及酸性的影响[J].石油学报(石油加工), 2011, 27(5):668-673. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=syxb-syjg201105002
YANG Ping, XIN Jing, LI Ming-feng, NIE Hong. Effect of Mo and W oxides on the structure and acidity of Y zeolite[J]. Acta Pet Sin, 2011, 27(5):668-673. http://www.wanfangdata.com.cn/details/detail.do?_type=perio&id=syxb-syjg201105002
|
[40] |
LIU H, SU L, WANG H, SHEN W, BAO X, XU Y. The chemical nature of carbonaceous deposits and their role in methane dehydroaromatization on Mo/MCM-22 catalysts[J]. Appl Catal A:Gen, 2002, 236(1/2):263-280. https://core.ac.uk/display/192001822
|
[41] |
ZHANG H, SHAO S, XIAO R, SHEN D, ZENG J. Characterization of coke deposition in the catalytic fast pyrolysis of biomass derivates[J]. Energy Fuels, 2014, 28(1):52-57. doi: 10.1021/ef401458y
|
[42] |
MA D, WANG D, SU L, XU Y, BAO X. Carbonaceous deposition on Mo/HMCM-22 catalysts for methane aromatization:A TP technique investigation[J]. J Catal, 2002, 208(2):260-269. http://cn.bing.com/academic/profile?id=88fb32c22f5481238dd3be4505c07dea&encoded=0&v=paper_preview&mkt=zh-cn
|