Synthesis of ZIF-8-coated Pt/SiO<sub>2</sub> by vapor deposition for alkyne semi-hydrogenation

LUO Gen; ZHANG Bin; YANG Xin-chun; WU Hui-bin; MENG Fan-chun; ZHAI Li-ming; QIN Yong

doi:10.1016/S1872-5813(21)60075-0

Volume 49 Issue 9

Sep. 2021

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Article Navigation > Journal of Fuel Chemistry and Technology > 2021 > 49(9): 1316-1325

LUO Gen, ZHANG Bin, YANG Xin-chun, WU Hui-bin, MENG Fan-chun, ZHAI Li-ming, QIN Yong. Synthesis of ZIF-8-coated Pt/SiO2 by vapor deposition for alkyne semi-hydrogenation[J]. Journal of Fuel Chemistry and Technology, 2021, 49(9): 1316-1325. doi: 10.1016/S1872-5813(21)60075-0

Citation:

LUO Gen, ZHANG Bin, YANG Xin-chun, WU Hui-bin, MENG Fan-chun, ZHAI Li-ming, QIN Yong. Synthesis of ZIF-8-coated Pt/SiO₂ by vapor deposition for alkyne semi-hydrogenation[J]. Journal of Fuel Chemistry and Technology, 2021, 49(9): 1316-1325. doi: 10.1016/S1872-5813(21)60075-0

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Synthesis of ZIF-8-coated Pt/SiO₂ by vapor deposition for alkyne semi-hydrogenation

doi: 10.1016/S1872-5813(21)60075-0

LUO Gen^{1, 2
,},
ZHANG Bin^{1
,
,},
YANG Xin-chun^{1, 2},
WU Hui-bin^{1, 2},
MENG Fan-chun^{1, 2},
ZHAI Li-ming^{1, 2},
QIN Yong^{1, 2}

1.
State Key Laboratory of Coal Conversion, Institute of Coal Chemistry, Chinese Academy of Sciences, Taiyuan 030001, China
2.
Center of Materials Science and Optoelectronics Engineering, University of Chinese Academy of Sciences, Beijing 100049, China

Funds: The project was supported by the National Natural Science Foundation of China (22072172, 21872160), the Youth Innovation Promotion Association CAS (2017204), and Natural Science Foundation of Shanxi Province (201901D211591), the National Science Fund for Distinguished Young Scholars (21825204)

Received Date: 2021-02-08
Rev Recd Date: 2021-03-29

Available Online: 2021-04-07

Publish Date: 2021-09-30

Abstract

Abstract

In this work, ZIF-8/Pt/SiO₂ catalysts were prepared by combining atomic layer deposition (ALD) and vapor phase conversion methods. First, Pt metal nanoparticles were deposited on SiO₂ nanowires by ALD. Then, ZnO was further deposited, also by ALD. Subsequently, the ZnO film was converted into ZIF-8 film by vapor phase crystallization to form a sandwich structure (ZIF-8/Pt/SiO₂). The microstructures of the catalysts were characterized by XRD, TEM, BET, IC-MS, XPS, and CO-DRIFT. It was shown that the Pt particles were highly dispersed on the SiO₂nanowires before and after coating with ZIF-8, and the ZIF-8 film was coated continuously on the entire catalyst with high conformity. The performance of the catalyst was studied by using the semi-hydrogenation of 1-heptyne as a probe reaction. The ZIF-8 film induces an electron density increase in the Pt component, leading to an increase of the olefin selectivity from 14% to 70% in the 1-heptyne hydrogenation reaction. A reduced thickness of the ZIF-8 film increases the catalytic activity but does not affect the selectivity of 1-heptylene.
- atomic layer deposition,
- vapor phase crystallization,
- ZIF-8 film,
- semi-hydrogenation

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References(38)

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